By Serena Ng And Ellen Byron 

Procter & Gamble Co. is dismantling a beauty business it aggressively built a decade ago, giving up on areas like salon products and designer perfumes that distracted from core areas and hurt its growth.

The world's largest consumer-products company said Thursday it would carve off brands including Wella shampoos, Clairol hair dye and CoverGirl makeup and merge them with Coty Inc. in a complicated $13 billion deal.

P&G spent about $80 billion over the past two decades scooping up brands including Gillette razors, Duracell batteries and Iams pet food, only to end up selling some of them to focus on boosting sales of Tide detergent, Pampers diapers and other mainstays.

The new round of divestitures is a remarkable reversal for Chief Executive A.G. Lafley, who returned to the company in 2013 to lead it out of a long slump. In his first stint running P&G from 2000 to 2009, Mr. Lafley pushed the company heavily into the beauty business, which he prized for its fatter profit margins and growth potential.

Under his leadership, P&G paid more than $10 billion for Wella and Clairol, bought a chain of boutique hair salons, and formed partnerships with designer brands like Valentino and Dolce & Gabbana to sell perfumes in high-end department stores, a departure from the long-honed strategy of mass marketing everyday staples.

But the company has decided it won't chase fashion trends anymore. Mr. Lafley is now preaching focus by exiting as many as 100 brands and reducing the company's nonmanufacturing workforce by about a third.

"P&G was looking to conquer the world of beauty but it went too far out of its comfort zone," said Carrie Mellage, vice president of consulting firm Kline & Co.'s consumer-products practice. She said there are few synergies between beauty products sold in high-end department stores and those sold at mass retailers.

P&G, General Electric Co. and some other American corporations are rushing to shed underperforming divisions and slim down after years of bulking up through acquisitions outside their core expertise. The change of heart among top executives is an admission that their companies had grown too big and bloated to manage effectively, which caused their stock prices to languish in recent years.

Meanwhile, the rise of activist investors empowered by big war chests and more-accommodating corporate governance rules has raised the stakes for companies that persistently turn in worse results than their peers. Three years ago, an assault by activist hedge-fund manager Bill Ackman helped crystallize discontent among investors in P&G, culminating in a decision to remove Chief Executive Bob McDonald.

The latest deal will involve transferring 43 P&G brands into a separate company that will merge with Coty, a New York-based company that makes Sally Hansen nail polish, Rimmel cosmetics and a range of perfumes. The beauty brands P&G is parting with have annual sales of $5.9 billion--more than a quarter of the $19.5 billion beauty division total for the year ended June 2014. (P&G hasn't reported results yet for its most recent fiscal year.) It would more than double the current size of Coty, which reported $4.6 billion in sales in its fiscal year ended June 2014, and will involve the transfer of around 10,000 P&G employees. Coty shares fell 4.7% on the news; Procter shares were flat.

The deal's final price and form haven't been settled, and it may not be completed until the second half of next year, P&G said. It likely will allow P&G shareholders to exchange their shares for shares in Coty or a new merged entity that will own the beauty brands of both firms. P&G also said it is aiming to return up to $70 billion to shareholders via dividends and share buybacks in the next four years.

In an interview, Coty Chairman Bart Becht, himself a former P&G employee, said his company had expressed interest in P&G's beauty assets as far back as last summer, when Mr. Lafley first mapped out plans to shed dozens of brands to focus on the 65 that account for almost all of the company's sales and profit.

P&G isn't entirely exiting beauty. It will keep its largest hair, skin and personal-care brands, which include Pantene shampoo, Olay facial moisturizers and SK-II luxury skin care. Sales of Pantene and Olay, however, have been weak in recent years and Olay has steadily lost market share. The two brands are the chief reasons why P&G's beauty unit has lagged behind other divisions.

Early on, as Mr. Lafley talked up the budding beauty business, brand managers were eager to apply P&G's rigorous consumer research and production prowess to the often inefficient practices common in beauty-industry product development and manufacturing.

"At the time, going after this business made all the sense in the world, " a former P&G employee said.

But a company adept at pitching products based on performance was suddenly trying to conquer categories won by the subtleties of fragrance, packaging and sexy image advertising.

P&G created sleek workspaces in New York and Geneva to dazzle beauty editors and entice prospective partners. Employees stumbled a decade ago by showing up at fashion events in navy sport coats and khakis, but later traded up to sharp suits and trendy heels.

"You were expected to look the part, and you were told if you didn't," another former P&G employee said.

Mr. Lafley's enthusiasm for the beauty business spilled into the way P&G marketed its other products. The packaging and advertisements of Crest toothpastes and whitening products increasingly touted beautiful smiles in addition to functional benefits. Dawn introduced dish soap that promised to improve "the look and feel of hands."

The company's instincts, however, proved wrong for the business. In 2008, P&G bought the Frederic Fekkai brand founded by the celebrity hairstylist, a pioneer of selling 7-ounce bottles of shampoo for more than $30 at retailers like Saks Fifth Avenue and Neiman Marcus. P&G expanded the Fekkai line to mass retailers like Target, despite protests from department stores that it would kill the allure, according to people familiar with the matter. Ultimately, Fekkai's sales dwindled and the brand was sold this year.

Other attempts to build scale across its beauty brands foundered, too. Some inside P&G hoped to find tie-ins between its mass brands and designer fragrances, including product placement of Pantene shampoo and CoverGirl makeup at Dolce & Gabbana and Gucci fashion shows, according to the former P&G employees. The fashion houses and some brand experts at P&G balked and ultimately the ideas were scratched. Instead, P&G's mass brands forged broader sponsorships with Fashion Weeks in Milan and New York and the Grammys.

At the highest levels, P&G executives struggled with how to manage and define the beauty business. At one point, P&G's beauty division included Gillette and Braun shaving gear, and brands were subdivided into "male" and "female" categories. That approach was scrapped after two years. For another period, the beauty brands were part of a group that included oral care and feminine-care products.

Over the past year, the 68-year-old Mr. Lafley concluded that P&G needed to focus more on brands that had clearly defined benefits, and not those whose sales were dictated by fashion trends.

"We start thinking we are a beauty company and we spend all our time at the Oscars or the Grammys or in Fashion Week, which now runs for months, and we don't stay focused on the consumer," he said at an analyst conference last year.

Write to Serena Ng at serena.ng@wsj.com and Ellen Byron at ellen.byron@wsj.com

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